HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylnaphthalene → HCID 86673229, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylnaphthalene | HCID 7002 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | HCID 86673229 | HCID 86673229 | 86.2% |
Reaction Steps
1-methylnaphthalene (142 mg), acryloyl chloride (100 mg), and aluminium chloride (150 mg) were reacted in carbon disulfide (0.5 mL) at from −20° C. to room temperature for 1 hour. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (169 mg) in a viscous liquid form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-1c0ca1fbcf0d427baee0ec4b9f6b74dc |
| Source note | uspto-grants-2015_01 |