HuagongsheHuagongshe Chemistry Print Report · For research reference only
Naphthalene → HCID 14606584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Naphthalene | HCID 931 | — |
| Reactant | trans-Crotonyl chloride | HCID 643131 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14606584 | HCID 14606584 | 64.3% |
Reaction Steps
Naphthalene (128 mg), crotonoyl chloride (124 mg), and aluminium chloride (180 mg) were reacted in dichloromethane (1.5 mL) at from −20° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (126 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-54a14fdd55934931b8db93cf312e7f57 |
| Source note | uspto-grants-2015_01 |