HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anisole → HCID 46913386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anisole | HCID 7519 | — |
| Reactant | (2E)-2-Methyl-2-butenoyl chloride | HCID 5325503 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 46913386 | HCID 46913386 | 28% |
Reaction Steps
Anisole (128 mg), tigloyl chloride (140 mg), and aluminium chloride (155 mg) were reacted in dichloromethane (1.5 mL) at from 0° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (63 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-ffa371fd5edf4817b2e522c2d8abfa6a |
| Source note | uspto-grants-2015_01 |