Ethylbenzene → HCID 21394659, compound

HRID 1428452Notes

Reaction equation

HRID 1428452 reaction equation
[CH2:1]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1)[CH3:2].[C:9](Cl)(=[O:12])[CH:10]=[CH2:11].[Cl-].[Al+3].[Cl-].[Cl-]>ClCCl>[CH2:1]([C:3]1[CH:8]=[CH:7][C:6]([C:9](=[O:12])[CH:10]=[CH2:11])=[CH:5][CH:4]=1)[CH3:2]

Participants

5

Reactant 3

HCID 7500EthylbenzeneHCID 13140Acryloyl chlorideHCID 6451240Aluminum(III) Chloride

Product 1

HCID 21394659HCID 21394659, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Ethylbenzene (0.5 mL), acryloyl chloride (120 mg), and aluminium chloride (199 mg) were reacted in dichloromethane (1.5 mL) at from 0° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (110 mg).

Workup

  1. additionThe resultant was treated in the same manner

Sources & evidence

ORD record
ord-9c231df82b8742af932ba7e906a376ab
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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