HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylbenzene → HCID 21394659, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylbenzene | HCID 7500 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21394659 | HCID 21394659 | — |
Reaction Steps
Ethylbenzene (0.5 mL), acryloyl chloride (120 mg), and aluminium chloride (199 mg) were reacted in dichloromethane (1.5 mL) at from 0° C. to room temperature for 4 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (110 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-9c231df82b8742af932ba7e906a376ab |
| Source note | uspto-grants-2015_01 |