HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Fluoronaphthalene → HCID 46913484, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Fluoronaphthalene | HCID 9450 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 46913484 | HCID 46913484 | 195% |
Reaction Steps
1-fluoronaphthalene (146 mg), acryloyl chloride (110 mg), and aluminium chloride (150 mg) were reacted in dichloromethane (1 mL) at from −15° C. to room temperature for 2 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (390 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937091B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-8b496dbe5910410590f9268d1b9a9f7b |
| Source note | uspto-grants-2015_01 |