Formaldehyde → HCID 70926653, compound

HRID 1428472Notes

Reaction equation

HRID 1428472 reaction equation
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][N:5]=1)(=[O:3])[CH3:2].[NH:10]1[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1.[CH2:16]=O>O1CCOCC1>[N:10]1([CH2:16][CH2:2][C:1]([C:4]2[CH:9]=[CH:8][CH:7]=[CH:6][N:5]=2)=[O:3])[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1

Participants

5

Reactant 3

HCID 712FormaldehydeHCID 8082PiperidineHCID 142862-Acetylpyridine

Product 1

HCID 70926653HCID 70926653, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

2-acetylpyridine (121 mg), piperidine (65 mg), and paraformaldehyde (36 mg) were reacted in dioxane (0.2 ml) at 150° C. for 2 hours.

Sources & evidence

ORD record
ord-ea2b346752a6426a8eba9d81ce6c9027
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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