Formaldehyde → HCID 46231510, compound

HRID 1428473Notes

Reaction equation

HRID 1428473 reaction equation
C([N:4]1[CH:9]=[CH:8][N:7]=[CH:6][CH2:5]1)(=O)C.[NH:10]([CH2:14][CH2:15][OH:16])[CH2:11][CH2:12][OH:13].[CH2:17]=O.O1[CH2:24][CH2:23][O:22]CC1>>[CH:5]1[N:4]=[CH:9][C:8]([C:23]([CH2:24][CH2:17][N:10]([CH2:14][CH2:15][OH:16])[CH2:11][CH2:12][OH:13])=[O:22])=[N:7][CH:6]=1

Participants

5

Reactant 4

HCID 712FormaldehydeHCID 8113DiethanolamineHCID 312751,4-DioxaneHCID 69349347HCID 69349347, compound

Product 1

HCID 46231510HCID 46231510, compound

Procedure

1-acetylpyrazine (122 mg), diethanol amine (105 mg), and paraformaldehyde (39 mg) were reacted in dioxane (0.2 ml) at 130° C. for 2 hours.

Sources & evidence

ORD record
ord-e868a0457a024006a4fb5301cabbb8ca
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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