Formaldehyde → HCID 70494583, compound

HRID 1428476Notes

Reaction equation

HRID 1428476 reaction equation
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)(=[O:3])[CH3:2].[CH3:10][N:11]1[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]1.[CH2:17]=O>O1CCOCC1>[CH3:10][N:11]1[CH2:16][CH2:15][NH:14][CH2:13][CH:12]1[CH2:17][CH2:2][C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)=[O:3]

Participants

5

Reactant 3

HCID 712FormaldehydeHCID 7410AcetophenoneHCID 531671-Methylpiperazine

Product 1

HCID 70494583HCID 70494583, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

Acetophenone (120 mg), N-methylpiperazine (100 mg), and paraformaldehyde (36 mg) were reacted in dioxane (0.2 ml) at 150° C. for 2 hours.

Sources & evidence

ORD record
ord-2e7e89be983b4118bcad75bd3b12fe59
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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