Formaldehyde → HCID 70926873, compound

HRID 1428480Notes

Reaction equation

HRID 1428480 reaction equation
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][N:5]=1)(=[O:3])[CH3:2].[C:10]1([NH:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[CH2:23]=O>O1CCOCC1>[C:17]1([N:16]([CH2:23][CH2:2][C:1]([C:4]2[CH:9]=[CH:8][CH:7]=[CH:6][N:5]=2)=[O:3])[C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=1

Participants

5

Reactant 3

HCID 712FormaldehydeHCID 11487DiphenylamineHCID 142862-Acetylpyridine

Product 1

HCID 70926873HCID 70926873, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

2-acetylpyridine (121 mg), diphenyl amine (169 mg), and paraformaldehyde (40 mg) were reacted in dioxane (0.2 ml) at 130° C. for 2 hours.

Sources & evidence

ORD record
ord-21205d5d080842b29d295755f7b318a2
Source dataset
uspto-grants-2015_01
Patent number
US08937091B2

Reaction notes

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