Formaldehyde → HCID 70926670, compound

HRID 1428483Notes

Reaction equation

HRID 1428483 reaction equation

[C:1]([C:4]1[CH:8]=[CH:7][S:6][CH:5]=1)(=[O:3])[CH3:2].[C:9]1([CH2:15][CH2:16][NH2:17])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.[CH2:18]=O>O1CCOCC1>[CH2:16]([NH:17][CH2:18][CH2:2][C:1]([C:4]1[CH:8]=[CH:7][S:6][CH:5]=1)=[O:3])[CH2:15][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

5

Reactant 3

HCID 712Formaldehyde

HCID 1001Phenethylamine

HCID 151161-(Thiophen-3-yl)ethanone

Product 1

HCID 70926670HCID 70926670, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

3-acetylthiophene (126 mg), phenylethyl amine (121 mg), and paraformaldehyde (40 mg) were reacted in dioxane (0.2 ml) at 130° C. for 2 hours.

Sources & evidence

ORD record: ord-a55413c59b4e4017b972b2e64f66f522
Source dataset: uspto-grants-2015_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08937091B2

Reaction notes

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