huagongshe.com
HRID1428695

反应详情

EQUATION

反应方程式

HRID 1428695 的结构方程式

REACTANTS

反应物

2
结构：[Ca]
HCID5460341

Calcium

Ca

2 次

结构：OC[C@H]1OC2C3[C@@H](CO)OC(O[C@H]4[C@H](O)[C@@H](O)[C@@H](O[C@H]5[C@H](O)[C@@H](O)[C@@H](O[C@H]6[C@H](O)[C@@H](O)[C@@H](O[C@H]7[C@H](O)[C@@H](O)[C@@H](O[C@H]8[C@H](O)[C@@H](O)[C@@H](O[C@H]9[C@H](O)[C@@H](O)C(OC1[C@H](O)[C@H]2O)O[C@@H]9CO)O[C@@H]8CO)O[C@@H]7CO)O[C@@H]6CO)O[C@@H]5CO)O[C@@H]4CO)[C@H](O)[C@H]3O
HCID44431027

未命名化合物

PRODUCTS

生成物

1
结构：OC[C@H]1OC2C3[C@@H](CO)OC(O[C@H]4[C@H](O)[C@@H](O)[C@@H](O[C@H]5[C@H](O)[C@@H](O)[C@@H](O[C@H]6[C@H](O)[C@@H](O)[C@@H](O[C@H]7[C@H](O)[C@@H](O)[C@@H](O[C@H]8[C@H](O)[C@@H](O)[C@@H](O[C@H]9[C@H](O)[C@@H](O)C(OC1[C@H](O)[C@H]2O)O[C@@H]9CO)O[C@@H]8CO)O[C@@H]7CO)O[C@@H]6CO)O[C@@H]5CO)O[C@@H]4CO)[C@H](O)[C@H]3O.[Ca]
HCID131732360

未命名化合物

PROCEDURE

实验过程

23 g of a calcium-based drier, Calcium CEM-ALL® 10% solution (OM Group, Inc.) was added to the above-noted γ-cylodextrin solution. A white precipitate formed upon addition of the drier. The mixture was stirred for at least 16 hours. The precipitate was filtered off under reduced pressure. The precipitate was dried under normal conditions at ambient temperature. The FTIR spectrum of the resultant inclusion complex is provided in FIG. 1(c).

WORKUP

后处理

  1. customA white precipitate formed upon addition of the drier
  2. filtrationThe precipitate was filtered off under reduced pressure
  3. customThe precipitate was dried under normal conditions at ambient temperature
  4. customThe FTIR spectrum of the resultant inclusion complex is provided in FIG. 1(c)