HRID1428780

反应详情

EQUATION

反应方程式

HRID 1428780 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

10% Palladium on carbon is added to a solution methyl 2-(3-fluoro-4-nitrophenyl)propanoate in methanol and the mixture is charged with H2 (g). After stirring the reaction mixture for 6 h, the mixture is filtered using celite packed filter and purified by column chromatography to obtain methyl 2-(4-amino-3-fluorophenyl)propanoate.

WORKUP

后处理

  1. additionthe mixture is charged with H2 (g)
  2. filtrationthe mixture is filtered
  3. filtrationpacked filter
  4. custompurified by column chromatography