HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68592566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 68592472 | HCID 68592472 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68592566 | HCID 68592566 | 99.4% |
Reaction Steps
Compound 7a (1.48 g, 2.68 mmol) was dissolved in 35 ml DCM. Triethylsilane (1.07 ml, 6.7 mmol) and 35 ml TFA were added and the mixture was stirred at RT for 45 minutes. The solvent was evaporated and co evaporated with toluene which gave the title product (1.32 g, 99%), MS (M+H)+496.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937080B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-d9200c526a2f4821a33935f4f2627ddd |
| Source note | uspto-grants-2015_01 |