HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylsilane → HCID 68590308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 68591327 | HCID 68591327 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 68590308 | HCID 68590308 | 130.2% |
Reaction Steps
Compound 16b (1.11 g, 1.9 mmol) was treated with triethylsilane (0.55 g, 4.75 mmol) and TFA (30 ml) according to the procedure described in Example 13 step b which gave the crude title compound, (1.3 g), (M+H)+526.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937080B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-b79ff7b0ab444534adae7db7c196cf24 |
| Source note | uspto-grants-2015_01 |