HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68592521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 68588666 | HCID 68588666 | — |
| Product | HCID 68592521 | HCID 68592521 | 110.8% |
Reaction Steps
Compound 17b (1.2 g, 2 mmol) was treated with triethylsilane (0.58 g, 5.0 mmol) and TFA (25 ml) according to the procedure described in Example 13 step b, which gave the crude title compound, (1.2 g), (M+H)+542.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937080B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-759135089656412b9a849d615d42b322 |
| Source note | uspto-grants-2015_01 |