HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68590874, compound → HCID 68590234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68590874 | HCID 68590874 | — |
| Catalyst | (1,3-Bis(2,4,6-trimethylphenyl)imidazolidin-2-ylidene)(dichloro)((2-((propan-2-yl)oxy)phenyl)methylidene)ruthenium | HCID 11763533 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 68590234 | HCID 68590234 | 76.1% |
Reaction Steps
The diolefin 17d (0.95 g, 1.49 mmol) was reacted with Hoveyda Grubbs 2nd generation catalyst (135 mg) in DCE (900 ml) according to the procedure described in Example 13 step d, which gave the title compound, (0.69 g, 76%), (M+H)+609.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08937080B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-8f2c788c443a472682d05458491e05d6 |
| Source note | uspto-grants-2015_01 |