HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 68532835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 68525508 | HCID 68525508 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68532835 | HCID 68532835 | 60% |
Reaction Steps
This compound has been obtained by reacting a solution of ethyl 2-(bis(2-(3,5-bis(methoxymethyl)-1H-pyrazol-1-yl)ethyl)amino)acetate (280 mg; 0.6 mmol) in dry THF (10 mL) with LiAlH4. The title compound was isolated following the same methodology above described for the synthesis of other (hydroxymethyl)pyrazoles (see example 6). Yield: 60% (170 mg, 0.4 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940273B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-7dbb0f4d6b0b4525a7af253cf134668a |
| Source note | uspto-grants-2015_01 |