HuagongsheHuagongshe Chemistry Print Report · For research reference only
Magnesium ethanolate → HCID 178525631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Magnesium ethanolate | HCID 164963 | — |
| Reactant | Propanedioic acid, monoethyl ester | HCID 3595298 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178525631 | HCID 178525631 | — |
Reaction Steps
To a stirred solution of monoethyl malonate 1(1.65 g, 12.5 mmol) in THF (25 mL) was added the magnesium ethoxide (0.61 g, 6.25 mmol). The reaction mixture was allowed to stir at rt for 5 h (until the solution become clear). The result solution was used for next step without any treatment.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940506B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-6bf30d76f105458abf336a2d91aa06a1 |
| Source note | uspto-grants-2015_01 |