Hydrochloric Acid → HCID 86679687, compound

HRID 1429342Notes

Reaction equation

HRID 1429342 reaction equation
O.Cl.C([O:5][CH:6](OCC)[CH2:7][N:8]([CH3:10])[CH3:9])C.[S:14]([O:17][S:18]([O-:20])=[O:19])([O-:16])=[O:15].[Na+].[Na+]>C(O)C>[S:14]([O:17][S:18]([OH:20])=[O:19])([OH:16])=[O:15].[CH3:9][N:8]([CH2:7][CH:6]=[O:5])[CH3:10]

Participants

6

Reactant 4

HCID 313Hydrochloric AcidHCID 962WaterHCID 24346Disodium disulfiteHCID 77163(2,2-Diethoxyethyl)dimethylamine

Product 1

HCID 86679687HCID 86679687, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Water (1 mL) and concentrated hydrochloric acid (2.4 mL) were added to dimethylaminoacetaldehyde diethyl acetal (2.00 g) and heating was carried out for 3 hours at 40° C. Sodium disulfite (3.0 M aqueous solution, 3.6 mL) and ethanol (10 mL) were added on an ice bath and stirring was performed for 1 hour and 30 minutes at room temperature. Filtration was carried out followed by concentration. The resulting residue was evaporated to dryness under reduced pressure at 60° C. to obtain the title compound (1.29 g).

Workup

  1. temperatureheating
  2. waitwas performed for 1 hour and 30 minutes at room temperature
  3. filtrationFiltration
  4. concentrationwas carried out followed by concentration
  5. customThe resulting residue was evaporated to dryness under reduced pressure at 60° C.

Sources & evidence

ORD record
ord-ebe259e170444d97a1b5a27d7dd2051f
Source dataset
uspto-grants-2015_01
Patent number
US08940725B2

Reaction notes

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