HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68233567, compound → HCID 67386725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68233567 | HCID 68233567 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67386725 | HCID 67386725 | 97% |
Reaction Steps
A solution of 30c (2.59 g, 8.75 mmol) in MeOH (100 mL) was hydrogenated using 10% Pd/C (0.93 g, 0.88 mmol) as catalyst at atmospheric pressure overnight. The catalyst was removed by filtration, and the solution was evaporated at reduced pressure to afford the desired product (2.27 g, 97% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940722B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-6625c93612de4e5d96df1cdbc823405a |
| Source note | uspto-grants-2015_01 |