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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1429397Generated: October 30, 2026

HCID 68233567, compound → HCID 67386725, compound

https://huagongshe.com/reaction/1429397

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68233567HCID 68233567—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 67386725HCID 6738672597%

Reaction Steps

A solution of 30c (2.59 g, 8.75 mmol) in MeOH (100 mL) was hydrogenated using 10% Pd/C (0.93 g, 0.88 mmol) as catalyst at atmospheric pressure overnight. The catalyst was removed by filtration, and the solution was evaporated at reduced pressure to afford the desired product (2.27 g, 97% yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08940722B2
Source datasetuspto-grants-2015_01
ORD IDord-6625c93612de4e5d96df1cdbc823405a
Source noteuspto-grants-2015_01