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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1429400Generated: November 1, 2026

HCID 86677164, compound → HCID 67382638, compound

https://huagongshe.com/reaction/1429400

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86677164HCID 86677164—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 67382638HCID 67382638—

Reaction Steps

A solution of 30f (crude 7.7 mmol) in MeOH (40 mL) was hydrogenated using 10% Pd/C (817 mg, 0.77 mmol) as catalyst at atmospheric pressure overnight. The catalyst was removed by filtration, and the solution was evaporated at reduced pressure to afford the crude desired product as yellow oil, which was used without further purification in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08940722B2
Source datasetuspto-grants-2015_01
ORD IDord-8433114c981241d9a09612356debbe2f
Source noteuspto-grants-2015_01