HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86677164, compound → HCID 67382638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86677164 | HCID 86677164 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67382638 | HCID 67382638 | — |
Reaction Steps
A solution of 30f (crude 7.7 mmol) in MeOH (40 mL) was hydrogenated using 10% Pd/C (817 mg, 0.77 mmol) as catalyst at atmospheric pressure overnight. The catalyst was removed by filtration, and the solution was evaporated at reduced pressure to afford the crude desired product as yellow oil, which was used without further purification in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940722B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-8433114c981241d9a09612356debbe2f |
| Source note | uspto-grants-2015_01 |