Potassium Carbonate → HCID 71269598, compound

Participants

Reaction Steps

To a solution of 30k (crude 1.58 mmol) in THF (10 mL) was added K2CO3 (436 mg, 3.16 mmol). The mixture was left to stir at rt until LC-MS analysis indicated the total consumption of the SM. Then the solid was removed by filtration and the solution was concentrated under reduced pressure to obtain the crude desired product. It was used without further purification in the next step.

Provenance & Evidence