HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 57420321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 58092771 | HCID 58092771 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57420321 | HCID 57420321 | — |
Reaction Steps
A mixture of (3R,7aR)-7a-methoxymethyl-3-trichloromethyl-tetrahydro-pyrrolo[1,2-c]oxazol-1-one (0.6 g) and 7M ammonia in methanol (6 ml) is stood at room temperature for 2 days in a sealed vessel. The reaction mixture is then evaporated to give the title compound as a pale yellow oil which is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940771B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-fb3f3ee3b8574d7587824541f9cee765 |
| Source note | uspto-grants-2015_01 |