HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 67507786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | Diethyl methylmalonate | HCID 11857 | — |
| Product | HCID 67507786 | HCID 67507786 | — |
Reaction Steps
Prepared according to general Procedure A using 4-fluoroaniline (18 g, 162 mmol), pyridine (13 mL, 162 mmol) and diethyl methylmalonate (28 mL, 162 mmol). After purification ethyl 3-(4-fluorophenylamino)-2-methyl-3-oxopropanoate was obtained. Mass Spectrum (ESI) m/e=240.1 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940724B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-eaef0a7dbaea42299548e8fac8519af7 |
| Source note | uspto-grants-2015_01 |