HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 67508161, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 67507786 | HCID 67507786 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67508161 | HCID 67508161 | — |
Reaction Steps
Prepared according to general Procedure B using ethyl 3-(4-fluorophenylamino)-2-methyl-3-oxopropanoate (20.0 g, 84 mmol) and NaOH (4.3 g, 81.5 mmol) in THF (50 mL). After purification 3-(4-fluorophenylamino)-2-methyl-3-oxopropanoic acid was obtained as a white solid. Mass Spectrum (ESI) m/e=212.2 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940724B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-dce9b91b62934b6bb4f12cd1591c2e8d |
| Source note | uspto-grants-2015_01 |