反应详情

Prepared according to Procedure J using 2-amino-4-fluorobenzoic acid (4.90 g, 31.6 mmol) and 1-(2-fluorophenyl)propan-1-one (3.70 g, 24.3 mmol) in phosphorous oxychloride (45.00 mL, 483 mmol) to afford product as a white solid upon purification by chromatography on silica gel. Mass Spectrum (ESI) m/e=290.0 (M+1).

1. customPrepared
2. customto afford product as a white solid
3. customupon purification by chromatography on silica gel