HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilic Acid → 4-Chloro-3-methyl-2-phenylquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilic Acid | HCID 227 | — |
| Reactant | 1-Phenyl-1-propanone | HCID 7148 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Product | 4-Chloro-3-methyl-2-phenylquinoline | HCID 12378945 | — |
Reaction Steps
Prepared according to Procedure J using anthranilic acid and propiophenone in phosphorous oxychloride to afford a colorless solid upon purification by chromatography on silica gel. Mass Spectrum (ESI) m/e=254.0 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940724B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-4d24cb1078714f448453cf066575ef47 |
| Source note | uspto-grants-2015_01 |