Anthranilic Acid → HCID 12378945, compound

HRID 1431273Notes

Reaction equation

HRID 1431273 reaction equation
[C:1](O)(=O)[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[NH2:4].[C:11]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)(=O)[CH2:12][CH3:13].P(Cl)(Cl)([Cl:23])=O>>[Cl:23][C:1]1[C:2]2[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:4]=[C:11]([C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[C:12]=1[CH3:13]

Participants

4

Reactant 3

HCID 227Anthranilic AcidHCID 71481-Phenyl-1-propanoneHCID 24813Phosphorus oxychloride

Product 1

HCID 12378945HCID 12378945, compound

Procedure

Prepared according to Procedure J using anthranilic acid and propiophenone in phosphorous oxychloride to afford a colorless solid upon purification by chromatography on silica gel. Mass Spectrum (ESI) m/e=254.0 (M+1).

Workup

  1. customPrepared
  2. customto afford a colorless solid
  3. customupon purification by chromatography on silica gel

Sources & evidence

ORD record
ord-4d24cb1078714f448453cf066575ef47
Source dataset
uspto-grants-2015_01
Patent number
US08940724B2

Reaction notes

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