HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 59631348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 1-(2-Fluorophenyl)propan-1-one | HCID 579399 | — |
| Reactant | 2-Amino-4,5-difluorobenzoic acid | HCID 735965 | — |
| Product | HCID 59631348 | HCID 59631348 | — |
Reaction Steps
Prepared according to Procedure J using 1-(2-fluorophenyl)propan-1-one and 2-amino-4,5-difluorobenzoic acid in phosphorous oxychloride to afford a colorless solid upon purification by chromatography on silica gel. Mass Spectrum (ESI) m/e=308.0 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940724B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-2e0550e4fd1843a187f3a21cf43154e3 |
| Source note | uspto-grants-2015_01 |