HCID 67507950, compound → HCID 59631447, compound

HRID 1431333Notes

Reaction equation

HRID 1431333 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9](=[O:17])[CH:10]([CH3:16])[C:11]([O:13]CC)=[O:12]>C1COCC1>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9](=[O:17])[CH:10]([CH3:16])[C:11]([OH:13])=[O:12]

Participants

3

Reactant 1

HCID 67507950HCID 67507950, compound

Product 1

HCID 59631447HCID 59631447, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The acid was prepared according to Procedure B using ethyl 3-(2-bromophenylamino)-2-methyl-3-oxopropanoate (2.7 g, 9.00 mmol) in THF (9.00 mL) to give 3-(2-bromophenylamino)-2-methyl-3-oxopropanoic acid. Mass Spectrum (ESI) m/e=272.0 (M+1).

Workup

  1. customThe acid was prepared

Sources & evidence

ORD record
ord-327bbffce83c4020ac1e353061b918ed
Source dataset
uspto-grants-2015_01
Patent number
US08940724B2

Reaction notes

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