HCID 67508600, compound → HCID 59631458, compound

HRID 1431337Notes

Reaction equation

HRID 1431337 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9](=[O:17])[CH:10]([CH3:16])[C:11]([O:13]CC)=[O:12]>C1COCC1>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][C:9](=[O:17])[CH:10]([CH3:16])[C:11]([OH:13])=[O:12]

Participants

3

Reactant 1

HCID 67508600HCID 67508600, compound

Product 1

HCID 59631458HCID 59631458, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The acid was prepared according to Procedure B using ethyl 3-(2-chlorophenylamino)-2-methyl-3-oxopropanoate (1.8 g, 7.04 mmol) in THF (7.0 mL) to give 3-(2-chlorophenylamino)-2-methyl-3-oxopropanoic acid. Mass Spectrum (ESI) m/e=228.1 (M+1).

Workup

  1. customThe acid was prepared

Sources & evidence

ORD record
ord-905c0a14835f4e96986333ab1f296992
Source dataset
uspto-grants-2015_01
Patent number
US08940724B2

Reaction notes

Loading…