HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59631518, compound → 3-(2-Chloro-5-fluorophenylamino)-2-methyl-3-oxopropanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59631518 | HCID 59631518 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-(2-Chloro-5-fluorophenylamino)-2-methyl-3-oxopropanoic acid | HCID 59631048 | — |
Reaction Steps
The acid was prepared according to Procedure B using ethyl 3-(2-chloro-5-fluorophenylamino)-2-methyl-3-oxopropanoate (5.0 g, 18.27 mmol) in THF (18.3 mL) to give 3-(2-chloro-5-fluorophenylamino)-2-methyl-3-oxopropanoic acid. Mass Spectrum (ESI) m/e=245.9 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940724B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-190bcf92d332477a9f9735ba54ad18b0 |
| Source note | uspto-grants-2015_01 |