HRID1431631

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC1(C)OB(c2cc([N+](=O)[O-])ccc2F)OC1(C)C

HCID3833297

2-(2-Fluoro-5-nitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

C12H15BFNO4

HCID59631108

未命名化合物

HCID59631513

2,4-Dichloro-5-fluoro-3-methylquinoline

C10H6Cl2FN

PRODUCTS

生成物

结构：Cc1c(-c2cc([N+](=O)[O-])ccc2F)nc2cc(F)ccc2c1Cl

HCID59631448

未命名化合物

PROCEDURE

实验过程

Essentially prepared according to Procedure F using a mixture of 2,4-dichloro-5-fluoro-3-methylquinoline and 2,4-dichloro-7-fluoro-3-methylquinoline (˜1:4 mixture) (690 mg, 3.00 mmol) and 2-(2-fluoro-5-nitrophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane to give 4-chloro-7-fluoro-2-(2-fluoro-5-nitrophenyl)-3-methylquinoline. Mass Spectrum (ESI) m/e=335.0 (M+1).

WORKUP

后处理

customEssentially prepared