HRID1431754

反应详情

EQUATION

反应方程式

HRID 1431754 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Prepared according to Procedure V using palladium (II) acetate (0.013 g, 0.057 mmol), tetramethyl t-butyl XPhos (0.082 g, 0.170 mmol), 4-(3-chloro-5-nitrophenyl)morpholine (0.275 g, 1.133 mmol), acetamide (0.080 g, 1.360 mmol), tripotassium phosphate (0.337 g, 1.587 mmol), and tert-butanol (2.5 mL) to afford N-(3-morpholino-5-nitrophenyl)acetamide. No purification was performed. Mass Spectrum (ESI) m/e=266.1 (M+1).

WORKUP

后处理

  1. customPrepared