HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-morpholino-5-nitrophenyl)isobutyramide → N-(3-amino-5-morpholinophenyl)isobutyramide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-morpholino-5-nitrophenyl)isobutyramide | HCID 67507653 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-(3-amino-5-morpholinophenyl)isobutyramide | HCID 67507609 | — |
Reaction Steps
Prepared according to Procedure V by stirring N-(3-morpholino-5-nitrophenyl)-isobutyramide (0.298 g, 1.016 mmol), 10% palladium on carbon (0.216 g, 0.203 mmol), and methanol (3 mL) for 30 minutes to afford N-(3-amino-5-morpholinophenyl)isobutyramide as a beige amorphous solid. Mass Spectrum (ESI) m/e=264.2 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08940724B2 |
| Source dataset | uspto-grants-2015_01 |
| ORD ID | ord-57f8484e41404b669a02a31655e9e988 |
| Source note | uspto-grants-2015_01 |