Water → Sebacic Acid
Reaction equation
[OH-:1].[Na+].[C:3]([OH:22])(=[O:21])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]CCCCCCCC.[OH2:23]>C(O)(C)C>[C:12]([OH:23])(=[O:1])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][C:3]([OH:22])=[O:21]Participants
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 70 °C
Procedure
10 g of Mg—Al hydroxide carbonate of the formula Mg6Al2(OH)16CO3 aq. (Pural MG 70, Sasol, Germany) are dispersed by stirring in 100 ml of deionized water at 70° C. for 15 minutes. Then a solution of 1.5 g of sebacic acid in 50 ml of deionized water is prepared with the addition of sodium hydroxide to a pH of approximately 9 and is added to the Mg—Al hydroxide carbonate suspension. Subsequently a solution of 2 g of stearic acid in a mixture of 50 ml of deionized water and 50 ml of isopropanol is prepared with the addition of sodium hydroxide to a pH of approximately 12 and heating to 70° C. and is added to the reaction mixture. The total mixture is stirred at 80° C. for 5 hours, and then the suspension is filtered, the solid product is washed repeatedly with deionized water and then the washed solid is dried in vacuo at 60° C.
Workup
- additionis added to the reaction mixture
- filtrationthe suspension is filtered
- washthe solid product is washed repeatedly with deionized water
- customthe washed solid is dried in vacuo at 60° C.
Sources & evidence
- ORD record
- ord-1bd83daeedab410ca7474538081017b7
- Source dataset
- uspto-grants-2009_11
- Patent number
- US07611812B2
Reaction notes
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