HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 86611311, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 68615631 | HCID 68615631 | — |
| Reactant | HCID 178418306 | HCID 178418306 | — |
| Product | HCID 86611311 | HCID 86611311 | — |
Reaction Steps
The title compound is prepared from 4-bromo-1-(m-chlorobenzensulfonyl)-2-(3,4-methylenedioxyphenyl)-pyrrole, tert-butyl lithium and DMF following the procedure of Example 3a. 1H-NMR (300 MHz, CDCl3): 9.89 (s, 1H); 8.08 (d, J=2.0 Hz, 1H); 7.6-7.5 (m, 1H); 7.4-7.25 (m, 4H); 6.8-6.7 (m, 1H); 6.65-6.55 (m, 1H); 6.55 (d, J=2.0, 1H); 6.05 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07612064B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-40e1f76dd25242579377ab9c18a04120 |
| Source note | uspto-grants-2009_11 |