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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1431973Generated: October 31, 2026

Dimethylformamide → HCID 86611311, compound

https://huagongshe.com/reaction/1431973

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamideHCID 6228—
ReactantHCID 68615631HCID 68615631—
ReactantHCID 178418306HCID 178418306—
ProductHCID 86611311HCID 86611311—

Reaction Steps

The title compound is prepared from 4-bromo-1-(m-chlorobenzensulfonyl)-2-(3,4-methylenedioxyphenyl)-pyrrole, tert-butyl lithium and DMF following the procedure of Example 3a. 1H-NMR (300 MHz, CDCl3): 9.89 (s, 1H); 8.08 (d, J=2.0 Hz, 1H); 7.6-7.5 (m, 1H); 7.4-7.25 (m, 4H); 6.8-6.7 (m, 1H); 6.65-6.55 (m, 1H); 6.55 (d, J=2.0, 1H); 6.05 (s, 2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07612064B2
Source datasetuspto-grants-2009_11
ORD IDord-40e1f76dd25242579377ab9c18a04120
Source noteuspto-grants-2009_11