HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 58962998, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 58962941 | HCID 58962941 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58962998 | HCID 58962998 | — |
Reaction Steps
Step AR2. To 3-chloro-4-(propylamino)benzonitrile (365 mg, 1.87 mmol) in MeOH (10 ml) was added bromine (300 mg, 1.87 mmol) in MeOH (2 mL) dropwise. After stirred for 30 minutes, the solvent was removed and crude 3-chloro-5-bromo-4-(propylamino)-benzonitrile was obtained (549 mg, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07612069B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-a02694901be1414fb64f5d685f378024 |
| Source note | uspto-grants-2009_11 |