HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 2-(but-3-enylamino)-6-methylisonicotinate → 2-But-3-enylamino-6-methyl-isonicotinic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 2-(but-3-enylamino)-6-methylisonicotinate | HCID 68545468 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | 2-But-3-enylamino-6-methyl-isonicotinic acid | HCID 68541987 | — |
Reaction Steps
A solution of 86 mg (0.33 mmol) 2-but-3-enylamino-6-methyl-isonicotinic acid tert-butyl ester in 2 ml TFA is stirred for 18 h and evaporated. The title compound thus obtained is used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07612055B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-47802633a74a409d87b9c0cdef71c7b0 |
| Source note | uspto-grants-2009_11 |