Tert-butyl 2-(but-3-enylamino)-6-methylisonicotinate → 2-But-3-enylamino-6-methyl-isonicotinic acid
反応式
C([O:5][C:6](=[O:19])[C:7]1[CH:12]=[C:11]([CH3:13])[N:10]=[C:9]([NH:14][CH2:15][CH2:16][CH:17]=[CH2:18])[CH:8]=1)(C)(C)C>C(O)(C(F)(F)F)=O>[CH2:15]([NH:14][C:9]1[CH:8]=[C:7]([CH:12]=[C:11]([CH3:13])[N:10]=1)[C:6]([OH:19])=[O:5])[CH2:16][CH:17]=[CH2:18]参加物
3
実験手順
A solution of 86 mg (0.33 mmol) 2-but-3-enylamino-6-methyl-isonicotinic acid tert-butyl ester in 2 ml TFA is stirred for 18 h and evaporated. The title compound thus obtained is used in the next step without further purification.
後処理
- customevaporated
出典と根拠
- ORDレコード
- ord-47802633a74a409d87b9c0cdef71c7b0
- 出典データセット
- uspto-grants-2009_11
- 特許番号
- US07612055B2
反応ノート
読み込み中…