Succinic anhydride → HCID 86052087, compound

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Reaction Steps

A mixture of 0.71 g (10 mmol) but-3-enylamine and 1.0 g (10 mmol) succinic anhydride in 10 ml DCM is stirred for 16 h. The mixture is poured into 25 ml 1N NaOH, washed with TBME, acidified with 6 ml 6N HCl, saturated with NaCl and extracted with THF/EtOAc twice. The combined organic layers are dried with sodium sulfate and evaporated to yield the title compound.

Provenance & Evidence