HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1432284Generated: November 1, 2026
HCID 22504411, compound → HCID 22504424, compound
https://huagongshe.com/reaction/1432284
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 22504411 | HCID 22504411 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 22504424 | HCID 22504424 | 49.3% |
Reaction Steps
To a solution of the compound obtained in Example 34 (4) (123 mg) in acetone (40 ml), manganese dioxide (1.86 g) was added and the mixture was stirred at −15 to 30° C. for-1 hour. The reaction solution was filtered through Celite and concentrated under reduced pressure to obtain 60 mg (49.3%) of the desired product as a yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07612070B2 |
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| Source dataset | uspto-grants-2009_11 |
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| ORD ID | ord-c3d215e93b0f43cd877000387b2f0884 |
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| Source note | uspto-grants-2009_11 |
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