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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1432284Generated: November 1, 2026

HCID 22504411, compound → HCID 22504424, compound

https://huagongshe.com/reaction/1432284

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22504411HCID 22504411—
CatalystHCID 178418406HCID 178418406—
SolventAcetoneHCID 180—
ProductHCID 22504424HCID 2250442449.3%

Reaction Conditions

Temperature7.5 °C

Reaction Steps

To a solution of the compound obtained in Example 34 (4) (123 mg) in acetone (40 ml), manganese dioxide (1.86 g) was added and the mixture was stirred at −15 to 30° C. for-1 hour. The reaction solution was filtered through Celite and concentrated under reduced pressure to obtain 60 mg (49.3%) of the desired product as a yellow powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07612070B2
Source datasetuspto-grants-2009_11
ORD IDord-c3d215e93b0f43cd877000387b2f0884
Source noteuspto-grants-2009_11