HCID 68897128, compound → HCID 68897867, compound

Participants

Reaction Steps

4-Benzyloxycarbonyl-1-[(2-{[N,N-dimethylaminoethyl]-amino }-pyrimidin-5-yl)-methyl]-3-(S)-methoxymethyl-piperazine-2-one (0.01 g, 0.02 mmol) and 10% Pd on carbon (0.01 g) are stirred in acetic acid (3 mL) under a hydrogen atmosphere for 18 h. The mixture is filtered through Celite@ and is evaporated to provide the intermediate title compound as a clear colorless oil (0.002 g). MS (ES), 323 [M+H]+.

Provenance & Evidence