HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-ethylpentane → (3S,5S)-3-(3-ethylpentyl)-3-methyl-5-phenylmorpholin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-ethylpentane | HCID 17763800 | — |
| Reactant | (5S)-3-methyl-5-phenyl-5,6-dihydro-2H-1,4-oxazin-2-one | HCID 57467834 | — |
| Product | (3S,5S)-3-(3-ethylpentyl)-3-methyl-5-phenylmorpholin-2-one | HCID 57467831 | — |
Reaction Steps
The title compound was prepared from (5S)-3-methyl-5-phenyl-5,6-dihydro-2H-1,4-oxazin-2-one (0.454 g, 2.39 mmol, see WO-A-02/051983) and 1-bromo-3-ethylpentane (see Bull. Soc. Chim. Fr., 1975, 201-205) according to the procedure outlined in Preparation 1. The total amount of compound synthesised was 0.07 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07612226B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-2f46e269f0094cd99ab77d7207e2bf0b |
| Source note | uspto-grants-2009_11 |