HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromo-2-nitrobenzene → 2-(6-Methoxy-3,3-dimethyl-3,4-dihydronaphthalen-2-yl)phenylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromo-2-nitrobenzene | HCID 11341 | — |
| Edukt | 7-Methoxy-2,2-dimethyl-3-(2-nitrophenyl)-1,2-dihydronaphthalene | HCID 23087552 | — |
| Edukt | 3-Bromo-7-methoxy-2,2-dimethyl-1,2-dihydronaphthalene | HCID 23087570 | — |
| Produkt | 2-(6-Methoxy-3,3-dimethyl-3,4-dihydronaphthalen-2-yl)phenylamine | HCID 23087497 | 53,5% |
Reaktionsschritte
Synthesized from 3-bromo-7-methoxy-2,2-dimethyl-1,2-dihydronaphthalene and 1-bromo-2-nitrobenzene according to an analogous synthetic method to Preparation Example 107 described below, 7-methoxy-2,2-dimethyl-3-(2-nitrophenyl)-1,2-dihydronaphthalene (1.4 g) was used according to an analogous synthetic method to Example 57 to provide the title compound (676 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07612114B2 |
| Quelldatensatz | uspto-grants-2009_11 |
| ORD ID | ord-9d3451f145e6432fa6898fbbb73474ec |
| Quellennotiz | uspto-grants-2009_11 |