4-Tert-Butylaniline → HCID 11577396, compound

Participants

Reaction Steps

The title compound was prepared using the procedure of Example 1C, substituting the product of Example 7B (0.1476 g, 0.450 mmol) for the product of Example 1B and substituting 4-aminophenyl trifluoromethyl sulphone (0.2571 g, 1.14 mmol) for 4-tert-butylaniline. MS (ESI+) m/z 536 (M+H)+, m/z 534 (M−H)−; 1H NMR (CD3OD) δ 7.73 (dd, J 4.7, 8.1, 1H), 7.99 (d, J 8.2, 1H), 8.12 (s, 1H), 8.19 (d, J 9.2, 2H), 8.38 (m, 3H), 8.46 (d, J 7.8, 1H), 8.92 (d, J 4.4, 1H).

Provenance & Evidence