4-Tert-Butylaniline → HCID 11504050, compound

Participants

Reaction Steps

The title compound was prepared using the procedure as described in Example 1C, substituting the product of Example 7B for the product of Example 1B, and substituting 4-trifluoromethoxy aniline for 4-tert-butylaniline. MS (DCI+) m/z 488 (M+H)+ (50%), m/z 309 (M-177)+ (100%); 1H NMR (DMSO-d6) δ 7.53 (d, J 8.5, 2H), 7.78 (dd, J 5.1, 7.2, 1H), 8.01 (m, 3H), 8.15 (s, 1H), 8.42 (d, J 8.1, 1H), 8.57 (d, J 7.1, 1H), 8.99 (d, J 4.7, 1H), 11.11 (s, 1H).

Provenance & Evidence