HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68983508, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57936549 | HCID 57936549 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 68983508 | HCID 68983508 | 190% |
Reaction Steps
To a mixture of 3-[2-(2-aminoethoxy)-4-methylsulfonyl-benzoylamino]-N-(5-chloropyridin-2-yl)pyridine-2-carboxamide (3.17 g, 6.5 mmol) and 10% MeOH/CH2Cl2 (250 mL) was added 5 N HCl. After stirring for 1 hour, the mixture was concentrated to give the desired product as a solid (3.25 g, 96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615568B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-2920abca8fe144e4880ca3b632d10e68 |
| Source note | uspto-grants-2009_11 |