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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1434834Generated: October 31, 2026

Hydrochloric Acid → HCID 68983508, compound

https://huagongshe.com/reaction/1434834

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 57936549HCID 57936549—
SolventDichloromethane methanolHCID 21226129—
ProductHCID 68983508HCID 68983508190%

Reaction Steps

To a mixture of 3-[2-(2-aminoethoxy)-4-methylsulfonyl-benzoylamino]-N-(5-chloropyridin-2-yl)pyridine-2-carboxamide (3.17 g, 6.5 mmol) and 10% MeOH/CH2Cl2 (250 mL) was added 5 N HCl. After stirring for 1 hour, the mixture was concentrated to give the desired product as a solid (3.25 g, 96%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07615568B2
Source datasetuspto-grants-2009_11
ORD IDord-2920abca8fe144e4880ca3b632d10e68
Source noteuspto-grants-2009_11