HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68983189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68982627 | HCID 68982627 | — |
| Product | HCID 68983189 | HCID 68983189 | 69% |
Reaction Steps
N-(5-Chloropyridin-2-yl)-3-[2-[(2R)-2-methyl-3-(2-propylimino)propoxy]-4-methylsulfonylbenzoylamino]-pyridine-2-carboxamide was treated with 1 N HCl and purified by HPLC (Vydac C18, 5-70% 0.1% TFA/CH3CN in 0.1% TFA/H2O; Rt: 27.6 m) to give the title compound as a solid (205 mg, 69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07615568B2 |
| Source dataset | uspto-grants-2009_11 |
| ORD ID | ord-2c2f587f2c554192a98c2d79f6acac4a |
| Source note | uspto-grants-2009_11 |